WLN-CO.W.32.1Determination of adsorbable organohalogen compounds (AOX) in water by means of micro-coulometryin-house method
Principle:The water sample is acidified with nitric acid to pH < 2. The organohalogen compounds are taken out of the water by shaking the sample with active carbon. The inorganic halogens are washed out by flushingwith an acidified sodium nitrate solution. Combustion of the hydrohalogens takes place in an oxygen flow. Absorption of the hydrohalogens is followed by the determination of halogen ions by means of micro-coulometry. The result is expressed as mass concentration of chloride.
Determination:Adsorbable organic halides
Performance characteristics:
Matrices qualified by the Dutch RvA:Drinking water, Groundwater
Reporting limit:0.15 umol/l, matrix dependent
Measurement uncertainty:50%
Sustainability:14 days , if conserved with HNO3
Sampling bottle:Glass , brown , 200 ml , conservation with HNO3 (fill up to cap)
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[ 16-08-2024 23:15:43 ]