WLN-CO.W.40.1Determination of different compounds by using LC-MSin-house method
Principle:The sample is, after acidification and addition of labeled internal standards, injected and analyzed by using high pressure liquid chromatography and accurate mass mass-selective detection. The surface ofthe peaks in the chromatogram is a measure of the concentration.
Determination:Metabolites
Performance characteristics:
Matrices qualified by the Dutch RvA (flexible scope):Drinking water, Groundwater, Surface water
Reporting limit:0.01 - 0.05 μg/l, parameter and matrix dependent
Measurement uncertainty:70%
Sustainability:6 days
Sampling bottle:Glass , brown , 100 ml (fill up to the neck of the bottle)
Parameters:
(RL = 0.01 μg/l)desamino-metamitron (not accreditated); pirimicarb desmethyl; pirimicarb desmethyl formamido; terbutylazine desethyl; 6-hydroxybentazon (not accreditated); 8-hydroxybentazon (not accreditated); 2-amino-N-isopropylbenzamide (not accreditated); prothioconazole-desthio (not accreditated)
(RL = 0.02 μg/l)spiromesifen metabolite M01
(RL = 0.05 μg/l)chloridazon-desphenyl; chloridazon-mehyl-desphenyl; dimethachlorosulfonic acid; dimethachloric acid; metazachlorosulfinic acid (geen Qf); metazachloric acid; metolachlorosulfonic acid; metolachloric acid
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[ 10-11-2023 10:58:56 ]