WLN-CO.W.05.4Determination of the mineral oil content by means of GC-FIDin-house method
Principle:The mineral oil is extracted from the water sample, after acidification and adding of sodium chloride. The extract is anhydrated and concentrated. A part of the concentrated extract is injected into a gaschromatograph. The oil is detected by means of a flame ionisation detector (FID). The total peak area of C10 up to and including C40 alkanes is a measure for the quantity of mineral oil.
Determination:Mineral oils
Performance characteristics:
Matrices qualified by the Dutch RvA:Wastewater, Drinking water, Groundwater, Surface water
Reporting limit:25 μg/l, matrix dependent
Measurement uncertainty:50%
Sustainability:28 days , if conserved with HNO3
Sampling bottle:Glass , brown , 200 ml , conservation with HNO3 (fill until marking)
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